楗敤姘翠腑涓夋隘鐢茬兎鍜屽洓姘寲纰崇殑椤剁┖姘旂浉鑹茶氨娴嬪畾娉?/p>
浣滆�咃細寮犲墠榫欙紝濮氱惁锛屾浌浜戯紝鎵僵涓?/p>
鎽樿锛氱洰鐨?/p>
寤虹珛娴嬪畾楗敤姘翠腑涓夋隘鐢茬兎鍜屽洓姘寲纰冲惈閲忕殑椤剁┖姣涚粏绠℃煴姘旂浉鑹茶氨娉曪紝鍚?/p>
鏃惰�冨療涓嶅悓鏉ユ簮楗敤姘翠腑姘豢鍜屽洓姘寲纰崇殑鍒嗗竷鐘跺喌銆?/p>
鏂规硶閲囩敤椤剁┖鑷姩杩涙牱鎶�鏈紝
鐢ㄧ壒寮?/p>
鎬?/p>
DB-624
姣涚粏绠℃煴姘旂浉鑹茶氨娉曟祴瀹氭按涓笁姘敳鐑峰拰鍥涙哀鍖栫⒊銆傜粨鏋滄爣鍑嗘洸绾跨殑鐩稿叧绯绘暟
涓?/p>
>0.999
锛?/p>
鐩稿鏍囧噯鍋忓樊涓?/p>
1.5%~8.3%
锛?/p>
涓夋隘鐢茬兎銆?/p>
鍥涙隘鍖栫⒊鐨勫钩鍧囧洖鏀剁巼涓?/p>
97.5%~103.3%
锛?/p>
涓夋隘鐢茬兎鐨勭嚎鎬ц寖鍥翠负
2.0~10.0渭g/L
锛?/p>
妫�鍑洪檺涓?/p>
0.02渭g/L
锛?/p>
鍥涙隘鍖栫⒊绾挎�ц寖鍥翠负
1.0~5.0渭g/L
锛?/p>
妫�鍑洪檺涓?/p>
0.003渭g/L
銆傜粨璁?/p>
璇ユ柟娉曠畝渚裤�佸揩閫燂紝鍏锋湁杈冨ソ鐨勭簿瀵嗗害涓庡噯纭害锛屽彲鐢ㄤ簬姘翠腑涓?/p>
姘敳鐑枫�佸洓姘寲纰崇殑娴嬪畾銆?/p>
鍏抽敭璇嶏細姘达紱椤剁┖姣涚粏绠℃煴姘旂浉鑹茶氨娉曪細涓夋隘鐢茬兎锛涘洓姘寲纰?/p>
姘豢鍜屽洓姘寲纰虫槸
GB5749-2006
銆婄敓娲婚ギ鐢ㄦ按鍗敓鏍囧噯銆嬩腑閲嶈鐨勫父瑙勬娴嬫寚鏍囥�?/p>
1974
骞寸編鍥界瀛﹀
Rook
鍜?/p>
Bellar
棣栧厛鍙戠幇鍔犳隘娑堟瘨鍚庢按涓儴鍒嗘尌鍙戞�у崵浠ｇ儍鍚噺浼氬崌楂橈紝鍙﹀
宸ヤ笟涓婂父鐢ㄦ隘浠裤�?/p>
鍥涙隘鍖栫⒊绛変綔涓哄師鏂欏拰婧跺墏锛?/p>
杩欎簺閮藉姞閲嶄簡姘豢鍜屽洓姘寲纰冲姘磋川閫犳垚鐨?/p>
姹℃煋銆傝祫鏂欒〃鏄庯紝姘豢銆佸洓姘寲纰冲叿鏈夎嚧鐧屻�佽嚧鐣搞�佽嚧绐佸彉浣滅敤锛岄暱鏈熸帴瑙﹀皢瀵逛汉浣撲骇鐢熶弗
閲嶅奖鍝嶃�?/p>
楗敤姘翠腑姘豢鍜屽洓姘寲纰崇殑涓昏娴嬪畾鏂规硶鏄《绌烘皵鐩歌壊璋辨硶锛?/p>
璇ユ硶鐩稿鍏朵粬鏂规硶
(
鍚?/p>
鎵崟闆嗐�佹恫
-
娑茶悆鍙栫瓑姘旂浉鑹茶氨娉?/p>
)
璁惧绠�鍗曘�佹搷浣滄柟渚裤�佸熀浣撳共鎵板皯銆傜瑪鑰呴噰鐢ㄨ繘鍙?/p>
Tekmar
椤剁┖鑷姩杩涙牱浠�?/p>
涓撻棬閽堝鎸ュ彂鎬ф湁鏈虹墿鍒嗘瀽鐨?/p>
DB-624
姣涚粏绠¤壊璋辨煴寤虹珛浜嗛ギ鐢ㄦ按涓笁姘?/p>
鐢茬兎鍜屽洓姘寲纰崇殑椤剁┖姘旂浉鑹茶氨娴嬪畾鏂规硶銆?/p>
1
鏉愭枡涓庢柟娉?/p>
1.1
浠櫒涓庤瘯鍓?/p>
V
arian
CP-3800
鍨嬫皵鐩歌壊璋变华
-
鐢靛瓙鎹曡幏妫�娴嬪櫒
(ECD)
锛?/p>
Agillent
DB-624
姣涚粏绠¤壊璋辨煴
(30m脳
0.32mm
锛?/p>
1.8渭m)
锛?/p>
Tekmar
7000
鍨嬮《绌鸿嚜鍔ㄨ繘鏍峰櫒銆備笁姘敳鐑枫�佸洓姘寲纰?/p>
(
鑹茶氨绾?/p>
)
銆?/p>
鐢查唶鍜屾姉鍧忚閰?/p>
(
鍒嗘瀽绾?/p>
)
鍧囪喘鑷浗鑽泦鍥㈠寲瀛﹁瘯鍓傛湁闄愬叕鍙?/p>
)
锛屾按
(
瓒呯函绾э紝缇庡浗
Millipore
鍏?/p>
鍙革紝鐢ㄥ墠鐓哺
10min
锛屾斁鍐?/p>
)
銆?/p>
1.2
椤剁┖
-
鑹茶氨鏉′欢
1.2.1
椤剁┖浠潯浠?/p>
椤剁┖骞宠 娓╁害涓?/p>
60
鈩冿紝骞宠 鏃堕棿涓?/p>
30min
锛屾牱鍝佺幆娓╁害涓?/p>
85
鈩冿紝浼犺緭
绾挎俯搴︿负
90
鈩冿紝杩涙牱鏃堕棿涓?/p>
0.5min
锛屾皵鐩歌壊璋卞惊鐜椂闂翠负
6min
銆?/p>
1.2.2
鑹茶氨鏉′欢
楂樼函
N
2
杞芥皵锛屾煴娴侀噺涓?/p>
5.0ml/min
锛氳繘鏍锋柟寮忎负椤剁┖鑷姩杩涙牱锛屽垎娴佹瘮涓?/p>
10
锛?/p>
1
锛涜繘鏍峰彛娓╁害涓?/p>
220
鈩冿紱妫�娴嬪櫒娓╁害涓?/p>
250
鈩冿紝灏惧惞姘旀祦閲忎负
30ml/min
锛涙煴娓╃▼搴忥細
鍒濇俯
40
鈩冿紝
1min
鍚庝互
13
鈩?/p>
/min
鍗囨俯鑷?/p>
85
鈩冦�?/p>
1.3
鏍囧噯婧舵恫閰嶅埗
1.3.1
鏍囧噯鍌ㄥ娑?/p>
鍑嗙‘绉板彇
0.8026g
涓夋隘鐢茬兎
(99.6%)
鍜?/p>
0.4020g
鍥涙隘鍖栫⒊
(99.5%)
鍒嗗埆鏀惧叆
瑁?/p>
鏈?/p>
灏?/p>
璁?/p>
鐢?/p>
閱?/p>
鐨?/p>
100ml
瀹?/p>
閲?/p>
鐡?/p>
涓?/p>
锛?/p>
瀹?/p>
瀹?/p>
鑷?/p>
鍒?/p>
搴?/p>
锛?/p>
姝?/p>
婧?/p>
娑?/p>
涓?/p>
P(CHCl
3
)=8.00mg/ml
銆?