瀹為獙涓�
姘旂浉鑹茶氨娉曟祴瀹氶娌圭簿涓杽鑽疯剳鐨勫惈閲?/p>
锛?/p>
Determination of menthol in
Essential balm
by gas chromatogaphy
锛?/p>
涓�銆佸疄楠岀洰鐨勶紙
Purpose
锛?/p>
1
銆佹帉鎻℃皵鐩歌壊璋卞嘲娴嬪畾鐨勬柟娉曞拰鍘熺悊锛?/p>
锛?/p>
To study the principles and procedures of GC for the assay of drugs
锛?/p>
2
銆佹帉鎻¤杽鑽疯剳鍚噺娴嬪畾鐨勬搷浣滄潯浠跺強瑕佺偣
(To grasp the conditions and points of determination of lambmirt in Fengyoujing)
3
銆佹帉鎻℃皵鐩歌壊璋辨潯浠剁殑寤虹珛涓庝紭鍖栨柟娉?/p>
锛?/p>
To grasp the method of establishing conditions and optional way
锛?/p>
浜屻�佸疄楠屽師鐞嗭紙
Principle
锛?/p>
鍐呮爣娉曠殑鐗圭偣锛氱粨鏋滀笉鍙楄繘杩涙牱閲忓拰鎿嶄綔鏉′欢鍙樺寲鐨勫奖鍝?/p>
鏍℃鍥犲瓙锛?/p>
/
/
s
s
R
R
A
C
f
A
C
飥?
寮忎腑锛?/p>
A
s
涓哄唴鏍囩墿鐨勫嘲闈㈢Н鎴栧嘲楂橈紱
C
s
涓哄唴鏍囩墿鐨勬祿搴︺�?/p>
A
R
涓哄鐓у搧鐨勫嘲闈㈢Н鎴栧嘲楂橈紱
C
R
涓哄唴鏍囩墿鐨勬祿搴︺�?/p>
鍚噺锛?/p>
/(
/
)
x
x
s
s
C
f
A
A
C
飥?/p>
飩?/p>
寮忎腑锛?/p>
A
x
涓轰緵璇曞搧锛堟垨鍏舵潅璐級鐨勫嘲闈㈢Н鎴栧嘲楂橈紱
C
x
涓轰緵璇曞搧锛堟垨鍏舵潅璐級鐨勬祿搴︺�?/p>
涓夈�佷华鍣ㄤ笌璇曞墏
浠櫒锛?/p>
Agilent 6820-GC
钖勮嵎鑴戝鐓у搧
鍥涖�佸疄楠屽唴瀹?/p>
锛堜竴锛夎壊璋辨潯浠?/p>
鑹茶氨鏌憋細
All
鐗?/p>
chECONOEC-1
鐔旇瀺姣涚粏绠℃煴
姘斿寲瀹ゆ俯搴︼細
200
飩?/p>
C
鏌辨俯锛?/p>
90
飩?/p>
C
鎴?/p>
100
飩?/p>
C
妫�娴嬪櫒娓╁害锛?/p>
200
飩?/p>
C
锛堜簩锛夋牎姝ｅ洜瀛愭祴瀹氾細
钖勮嵎鑴戝鐓у搧
50mg
鍐呮爣姝ｈ緵閱?/p>
100
飦?/p>
L
瀹氬鑷?/p>
10mL