榫欐簮鏈熷垔缃?/p>
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澶忎經濉旇嫹鐨勭數鍠烽浘鐢电瑁傝В瑙勫緥瑙ｆ瀽
浣滆�咃細寮犳灄娴?/p>
鏉庡簡鍥?/p>
鏉ユ簮锛氥�婁腑鍥藉尰鑽瀛︺�?/p>
2016
骞寸
07
鏈?/p>
[
鎽樿
]
鐩殑鐮旂┒澶忎經濉旇嫹鐨勮川璋卞绾ц瑙ｈ繃绋嬶紝鎺㈣璐ㄨ氨鎶�鏈湪榛勯叜纰抽厫涓殑搴旂敤瑙勫緥銆?/p>
鏂规硶搴旂敤鐢靛柗闆剧數绂伙紙
ESI
锛夌粨鍚堜覆鑱旇川璋憋紙
MSI
锛夋妧鏈紝瀵归粍閰⒊閰愬寲鍚堢墿澶忎經濉旇嫹鍦?/p>
ESI-
MS/MS
璐ㄨ氨涓殑瑁傝В瑙勫緥杩涜鐮旂┒銆傜粨鏋滃浣涘鑻峰湪璐熺瀛愭ā寮忎笅锛屽叾鍑嗗垎瀛愮瀛?/p>
m/
z
563
澶?/p>
绾ц川璋卞浘涓富瑕佸嚭鐜?/p>
[M-H-120]
銆?/p>
[M-H-90]
銆?/p>
[M-H-120-90]
銆?/p>
[M-H-120-60]
鍜?/p>
[M-H-120-90=C0]
绛夌瀛愮鐗囥�傜粨璁哄浣涘鑻峰湪
ESI-MS/MS
璐ㄨ氨涓殑瑁傝В琛屼负绗﹀悎榛勯叜纰抽厫鐨勮瑙ｈ寰嬶紝鏈夊埄
浜庡埄鐢ㄨ川璋辨妧鏈鍚勭榛勯叜纰宠嫹绫诲寲鍚堢墿鎵�鍚硸鍩虹绫昏繘琛屽垎鏋愬拰鐮旂┒銆?/p>
[
鍏抽敭璇?/p>
]
澶忎經濉旇嫹锛涚數鍠烽浘鐢电璐ㄨ氨锛涢粍閰⒊鑻凤紱瑁傝В锛涗覆鑱旇川璋?/p>
榛勯叜纰宠嫹绫诲寲鍚堢墿浠婂勾鏉ョ爺绌惰秺鏉ヨ秺娣卞叆锛屽凡缁忓舰鎴愪竴涓緝澶х殑浣撶郴锛屼絾鏄湁鍏宠绫诲寲鍚?/p>
鐗╃壒鍒槸澶忎經濉旇嫹鐨勬尝璋卞瑙勫緥鏂归潰杈冨皯瑙佷笓闂ㄧ殑鐮旂┒鎶ラ亾銆傚浣涘鑻锋槸浠庤眴绉戞鐗╁箍閲戦挶鑽?/p>
[Desmodiumstyracifolium
锛?/p>
Osh.
锛?/p>
Merr.]
鐨勫共鐕ュ湴涓婇儴鍒嗗垎绂绘墍寰椼�傚浣涘鑻锋槸涓�绉嶅吀鍨嬬殑榛勯叜
纰宠嫹绫诲寲鍚堢墿锛屽垎瀛愮粨鏋勪腑鍚屾椂鍚湁涓�涓垔绯栧拰涓�涓繁绯栵紝缁撴瀯濡傚浘
1
鎵�绀恒�備负浜嗘帉鎻″浣涘
鑻风殑
ESI-MS
纰庣墖绂诲瓙鐗瑰緛鍙婂熀鏈瑙ｈ寰嬶紝鏈枃閲囩敤
ESI-MS
瀵瑰浣涘鑻风殑璐ㄨ氨琛屼负杩涜浜?/p>
鐮旂┒锛屼负妞嶇墿绛夊鏉傛満浣撲腑鐥曢噺澶忎經濉旇嫹鐨勫揩閫熺洿鎺ュ垎鏋愭彁渚涗簡鍓嶆彁鍜屽熀纭�锛屽浜庡揩閫熷彂鐜板拰
閴村畾澶忎經濉旇嫹杩欑被纰宠嫹绫诲寲鍚堢墿鍏锋湁涓�瀹氱殑鎸囧鎰忎箟銆?/p>
1
浠櫒涓庤瘯鑽?/p>
Thermo LCQ FLEET
璐ㄨ氨浠喘鑷編鍥?/p>
Thremo
鍏徃銆傞厤缃湁
ESI
婧愶紝鍥涚骇鏉嗙瀛愰槺璐ㄩ噺鍒?/p>
绂诲櫒锛?/p>
Xcalibur
宸ヤ綔杞欢銆?/p>
TGL-16
鍙板紡楂橀�熺蹇冩満璐嚜婀栧崡鏄熺绉戝浠櫒鏈夐檺鍏徃锛?/p>
Milipak
绾按杩囨护鍣ㄨ喘鑷編鍥?/p>
Milipore
鍏徃锛涘浣涘鑻凤細鑷埗
[
涓鸿眴绉戞鐗╁箍閲戦挶鑽?
Desmodiumstyracifolium
锛?/p>
Osh.
锛?/p>
Merr.
鐨勫共鐕ュ湴涓婇儴鍒?/p>
]
锛涜壊璋辩函璐嚜寰峰浗
Sigma
鍏徃銆傝壊璋辩函
鐢查唶锛岀函鍖栨按锛屽叾浣欒瘯鍓備负鍒嗘瀽绾�?/p>
2
鏂规硶涓庣粨鏋?/p>
2.1
鏍峰搧澶勭悊鍙婅壊璋辨潯浠?/p>
绉板彇閫傞噺澶忎經濉旇嫹鐢ㄧ敳閱囨憾瑙ｏ紝绋�閲婅嚦绾?/p>
l渭g/mL
锛岀粡
0.22渭m
寰瓟婊よ啘杩囨护鍚庯紝鐢?/p>
300渭L
骞冲彛杩涙牱鍣ㄩ噰闆嗘牱鍝侊紝鍦ㄥ井閲忚繘鏍锋车鐨勬帹鍔ㄤ笅锛屼互
10渭L
/mL
娴侀�熼�氳繃姣涚粏绠¤繘鍏ヨ川璋憋紝杩炵画
杩涙牱锛岃皟鑺傝川璋辨潯浠讹紝杩涜澶氱骇璐ㄨ氨妫�娴嬨�?/p>
2.2
璐ㄨ氨鏉′欢